Thank you again if you responded to my previous emails.
I did cf again and then expinstall. It seems if you changed connections or
preamps when changing probes you have to do expinstall.
I used iconnmr and got some nice spectra.
Thank you, thank you, thank you.
Jay
Jay Shore
Associate Professor
Chemistry & Biochemistry & Physics
Avera Health & Science 355, Box 2202
Brookings, SD 57007
P: (605) 688-6356
SDState.edu<
https://www.sdstate.edu/>
> From: main_at_ammrl.groups.io on behalf of Shore, Jay via groups.io
> Date: Tuesday, June 18, 2024 at 1:24 PM
> To: main_at_ammrl.groups.io <main_at_ammrl.groups.io>
> Subject: Re: [AMMRL] edprosol conner
Thank you to everyone who responded to my original email.
I feel like this group has my back.
I apologize for not including more information.
Our system is an Avance II running Topspin 2.1
I did use edhead and it is the correct probe
When saving using setprosol I told it to save to all solvents
The “ignore proscol parameters” switch in ICONNMR was NOT activated
I was making the mistake of setting up a run in iconnmr and before running
it checking the parameters. I also made sure to save the parameters to the
probe when using setprosol and saving for all solvents.
Where it stands now.
I can get a great 1H spectrum using iconnmr or topspin.
I can NOT get a good 13C spectrum using iconnmr. If I go to the iconnmr created
spectrum, type “ii” and then run in topspin, there is still no signal.
I do have a file that has a beautiful 13C spectrum. If I go to it and type “ii”
and run in topspin, I get another beautiful spectrum.
I compared the parameters in eda line by line for the good and bad spectra
and I do not see any difference.
If I go to the spectrum created by iconnmr and type “edsp”
I get “Some routing parameters in the file ‘acqu’ are
not consistent with parameters saved in the file ‘specpar’.
Acquistion will not work if you do not save the correct routing.”
I also get “inconsistent observe routing for channel 1” I
do not get these warnings if I go to the files with the nice spectra.
Does anyone have any ideas.
Thank you all in advance.
Jay
Jay Shore
Associate Professor
Chemistry & Biochemistry & Physics
Avera Health & Science 355, Box 2202
Brookings, SD 57007
P: (605) 688-6356
SDState.edu<
https://www.sdstate.edu/>
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Received on Tue Jun 18 2024 - 13:08:01 MST