Maybe you coved this precviously. Did you do a cf command? You can set
the routing there.
Marcus
On Tue, Jun 18, 2024, 2:24 PM Shore, Jay <jay.shore_at_sdstate.edu> wrote:
>
>
> Thank you to everyone who responded to my original email.
> I feel like this group has my back.
> I apologize for not including more information.
> Our system is an Avance II running Topspin 2.1
>
> I did use edhead and it is the correct probe
> When saving using setprosol I told it to save to all solvents
> The “ignore proscol parameters” switch in ICONNMR was NOT activated
>
> I was making the mistake of setting up a run in iconnmr and before running
> it checking the parameters. I also made sure to save the parameters to the
> probe when using setprosol and saving for all solvents.
>
> Where it stands now.
>
> I can get a great 1H spectrum using iconnmr or topspin.
>
> I can NOT get a good 13C spectrum using iconnmr. If I go to the iconnmr
> created spectrum, type “ii” and then run in topspin, there is still no
> signal.
>
> I do have a file that has a beautiful 13C spectrum. If I go to it and type
> “ii” and run in topspin, I get another beautiful spectrum.
>
> I compared the parameters in eda line by line for the good and bad spectra
> and I do not see any difference.
>
> If I go to the spectrum created by iconnmr and type “edsp” I get “Some
> routing parameters in the file ‘acqu’ are not consistent with parameters
> saved in the file ‘specpar’. Acquistion will not work if you do not save
> the correct routing.” I also get “inconsistent observe routing for channel
> 1” I do not get these warnings if I go to the files with the nice spectra.
>
> Does anyone have any ideas.
>
> Thank you all in advance.
>
> Jay
>
> *Jay Shore*
> *Associate Professor*
> *Chemistry & Biochemistry & Physics*
>
> Avera Health & Science 355, Box 2202
> Brookings, SD 57007
>
> *P:* (605) 688-6356
> SDState.edu <https://www.sdstate.edu/>
>
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Received on Tue Jun 18 2024 - 12:08:25 MST