I ran 35Cl experiments on BBO probe with good tuning. The trick is the tuning
for 35Cl, if you cannot tune 35Cl with ATM.
Best,
Tianzhi
________________________________
> From: main_at_ammrl.groups.io on behalf of Wendy Breyer via groups.io
> Sent: Tuesday, April 9, 2024 2:49 PM
> To: main_at_ammrl.groups.io <main_at_ammrl.groups.io>
> Subject: [AMMRL] Chlorine NMR for trace compounds in bulk Cl- electrolyte?
Hi all,
I'm looking for some advice on the feasibility of some proposed experiments.
A user here would like to do Cl-NMR on aqueous electrolyte solutions. Specifically,
he would like to check for small amounts of OCl- and dissolved Cl2 in the presence
of 3M MgCl2. After searching the literature, I have been unable to locate any
publications that include similar experiments so I suspect that his proposed
experiments are not feasible... but my knowledge of NMR is superficial at best.
I'd be very interested in hearing from those with more experience whether these
experiments are possible. (For context, we have a 400 MHz Avance III HD with a
room temperature, broadband probe.)
Thanks for any input!
Wendy
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Received on Wed Apr 10 2024 - 09:15:28 MST