We're revamping and/or putting in place various policies/procedural documents
now that we have moved on from the Era of the Flood and into the Era of
Shiny New NMRs.
I'm curious what kind of specific guidelines you have in place for variable
temperature NMR?
*
Do you require a specific grade of NMR tube?
*
New NMR tubes?
*
What buffer do you allow between the solvent freezing/boiling point and the
target temperature? 10, 15, 20 degrees?
*
Anything else I'm missing?
Thanks in advance!
Ken Sharp-Knott
Manager of Analytical Services and the NMR Facility
Department of Chemistry
Virginia Tech
(540)267-6502 (Cell)
(540)231-0885 (Office)
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Received on Mon Oct 20 2025 - 07:47:05 MST