Re: [AMMRL] can get signal under nmrsu but not under a different user

From: Delk, Michael Joseph via groups.io <mid15=pitt.edu_at_groups.io>
Date: Tue, 25 Mar 2025 19:52:31 +0000

Did someone somehow change permissions on the acqu data files etc?

Mike Delk
University of Pittsburgh
School of Medicine
Department of Structural Biology
412.370.0066
________________________________
> From: main_at_ammrl.groups.io on behalf of Michael Groves via groups.io
> Sent: Tuesday, March 25, 2025 3:44:15 PM
> To: main_at_ammrl.groups.io <main_at_ammrl.groups.io>
> Subject: Re: [AMMRL] can get signal under nmrsu but not under a different user

That's a weird one. Are there multiple users that it's failing for or is it
just the one that can't get it to work? Are all the numbers in the dataset
correct--are there pulse lengths and pulse powers set, for example?

One thing I might check would be to see if the user is a member of either the
nmr users or the nmrsu groups. Maybe there's some weird permission thing going
on where if that user isn't a part of one of those groups they don't have
permission to write to the topspin data directory? Do you see any FID being
acquired or is the display always blank? Can you see anything in gs mode?
And can they acquire anything else--13C for example?

Cheers,
Mike

On Tuesday, March 25, 2025 at 01:25:50 PM MDT, Brian Antalek via groups.io wrote:


I am running TopSpin 3.2 on an AVII 300 MHz system under the nmrsu user.
Manual operation and iconnmr automation work fine.
But, when I switch to a different user, I cannot obtain 1H signal. It tunes
ok to 1H and locks and shims fine on D2O, but there is no acquired signal.

Before I switched to a different user, I exited TopSpin. I also successfully
ran ii when I restarted TopSpin in the other user.

Has anyone ever seen this? Does anyone have a remedy?

thanks
Brian


Brian Antalek
Bausch + Lomb, Inc.
1400 N. Goodman Street
Rochester, NY 14609

http://www.bausch.com
brian.antalek_at_bausch.com

(585) 752-8452 mobile




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Received on Tue Mar 25 2025 - 12:56:45 MST

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