Re: [AMMRL] 1H-19F HOESY setup tips?

From: Spin-Doc <bert.heise_at_spin-doc.net>
Date: Mon, 3 Mar 2025 22:51:55 +0100
Hi,

Before trying the way less sensitive HOESY did you try the way more sensitive H/F- (and/or F/H) 
HETCOR experiments on a compound showing a strong H-F coupling to make sure all tuning,
filters etc. are correct? Then try HOESY on the same compound - it shouldshow a strong NOE. O
Only then go to more “interesting” samples.

Good luck,
Bert

-> Sent via mobile <-

Spin-Doc 
Magnetic resonance equipment, service, training & more
Dr. rer. nat. Bert Heise
Owner, applications scientist
Kiefernweg 13
58239 Schwerte
Germany
Mail: bert.heise_at_spin-doc.net
Phone: +49-171-5135315

Representing MestreLab, Stelar & Barthel HF


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Received on Mon Mar 03 2025 - 13:53:27 MST

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