silylating glass NMR tubes

From: charlie dickinson <lcd_at_mail.pse.umass.edu>
Date: Wed, 31 Mar 2004 16:46:17 -0500

I have a user who is afraid his 200ug of preciously isolated
unknown agent extracted from Clostridia is absorbed on glass.
I can go the Teflon liner route, but at pretty big s/n expense.

I know there are methods of silylating interiors of normal
NMR tubes, but have never done it, nor do I find it in my
catalogues. What's the sources/technique?

pax

Charlie Dickinson

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Received on Wed Mar 31 2004 - 19:49:18 MST

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