Dear Jay,
What could have happened is that you saved the pulse parameters to one solvent.
Make sure you have these parameters copied properly to the solvent used in
your IconNMR experiments.
Jochem
> From: main_at_ammrl.groups.io On Behalf Of Schmieder, Peter
> Sent: Monday, June 17, 2024 9:19 AM
> To: main_at_ammrl.groups.io
> Subject: Re: [AMMRL] edprosol conner
Dear Jay,
two things to check come to my mind. The trivial test is to execute
“getprosol” in topspin in a suitable dataset and see
whether this works. Hard to imagine that it does not, but it is better
to check that.
In iconnmr there is the option in configuration/master switches to activate
“ignore prosol parameters”.
Maybe your datasets have all the correct pulses for the old probe, so you
never noticed that prosol was not used. After activating the prosol in
iconnmr it may work – if the “ignore” was in fact activated.
Best
Peter
> Von: main_at_ammrl.groups.io Im Auftrag von Shore, Jay
> Gesendet: Sonntag, 16. Juni 2024 22:20
> An: main_at_ammrl.groups.io<mailto:main_at_ammrl.groups.io>
> Betreff: [EXT] [AMMRL] edprosol conner
Okay … I am at my wits’ ends … again … which
was not a very for trip for me … seems like I am always in the neighborhood.
I changed probes on our Avance 600 from a PATXI to PABBO so that we could do
a wider range of nuclei (e.g., Pt).
Unfortunately, the bbo probe has never been calibrated (power and pulse lengths).
So, I went about calibrating and thought that as long as I saved the new power
levels and pulse lengths in the prosol file that they would show up when I went
to iconnmr. That is what the manual says. I saved the parameters in the prosol
file and saved it for the probe (all solvents). Then, I started iconnmr (routine
spectroscopy), set up an experiment, looked at the parameters (for pulse length
and power) and they were not the same as in the prosol file. Does anyone have
any ideas of what I am missing? Does anyone have a good reference for calibrating
deuterium power and pulse lengths or changing probes.
I would appreciate any advice.
Thank you.
Jay
Jay Shore
Associate Professor
Chemistry & Biochemistry & Physics
Avera Health & Science 355, Box 2202
Brookings, SD 57007
P: (605) 688-6356
SDState.edu<
https://www.sdstate.edu/>
-=-=-=-=-=-=-=-=-=-=-=-
Groups.io Links: You receive all messages sent to this group.
View/Reply Online (#1338): https://urldefense.com/v3/__https://ammrl.groups=
.io/g/main/message/1338__;!!PvDODwlR4mBZyAb0!X1hC8FhAhW5VSJJ1GRulqHLyiJyOae=
_JHExidrqv6UwW8CfJef13rZ6zM4rpO_F_dBDUW-2aGuizjsbIykT7rn6l9_uQ$
Mute This Topic: https://urldefense.com/v3/__https://groups.io/mt/106713226=
/7559972__;!!PvDODwlR4mBZyAb0!X1hC8FhAhW5VSJJ1GRulqHLyiJyOae_JHExidrqv6UwW8=
CfJef13rZ6zM4rpO_F_dBDUW-2aGuizjsbIykT7ro-Ronqq$
Group Owner: main+owner_at_ammrl.groups.io
-=-=-=-=-=-=-=-=-=-=-=-
Received on Mon Jun 17 2024 - 07:12:21 MST