Hello,
I believe those ending with _bbhd are the ones with broadband homodecoupling
using the BIRD block during acquisition time. They do not necessarily have
the "perfect" BIRD blocks in the middle of the sequence, which are placed
there to re-invert the desired 1JCH while 2JHH are inverted - I guess we are
talking about the Perfect 1JCH-resolved HSQC experiment
As far as I know this pulse sequence from the JMR paper from Parella is not
on the Bruker library, but they always publish the pp codes in the Supp. Info.
I tested the sequence years ago with success, I could offer some advice setting
it up on Topspin if needed.
Cheers,
Josep.
_____________________________________
Josep Saurí, PhD
NMR Spectroscopist | Research Scientist
Organic & Pharmaceutical Chemistry Department
IQS School of Engineering
Via Augusta 390, 08017 Barcelona
josep.sauri_at_iqs.url.edu
ORCID<
https://orcid.org/0000-0002-2706-2426 | Personal website<
https://jsaurinmr.wordpress.com/>
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Received on Thu Aug 29 2024 - 11:38:52 MST