Re: [AMMRL] Perfect 1JCH-resolved HSQC

From: Hansen, Alex <hansen.434_at_osu.edu>
Date: Thu, 29 Aug 2024 17:58:10 +0000

The HSQC sequences you're looking for end with _bbhd

hsqcetgpsisp2.2_bbhd

For instance.

Alex

________________________________
> From: main_at_ammrl.groups.io on behalf of xie via groups.io
> Sent: Thursday, August 29, 2024 1:07:30 PM
> To: main_at_ammrl.groups.io <main_at_ammrl.groups.io>
> Subject: [AMMRL] Perfect 1JCH-resolved HSQC

Dear colleagues,

We would like to measure 1JCH coupling constants along F1 direction by
using a hsqc experiment, for a comparison with those we obtained along
F2 in a non-decoupled hsqc spectrum. Parella et al. published in 2017
a very impressive method, with double BIRDs to get rid of the
influence on the lineshape due to nJHH (N. Marcó et al. JMR 276,
37–42). Maybe someone knows if this pulse sequence is already included
in the Bruker pulse program library or not and if yes, please kindly
tell us its name in the Bruker pulse program library.

Many thanks and best wishes,

Xiulan


********************************************
Dr. Xiulan Xie (sie/ihr)
Serviceabteilung NMR-Spektroskopie
Fachbereich Chemie
Philipps-Universität Marburg
Hans-Meerwein-Strasse 4
35032 Marburg, Germany
Phone: +49-6421-2825520
Fax: +49-6421-2825422
Email: xie_at_staff.uni-marburg.de
*******************************************


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Received on Thu Aug 29 2024 - 10:58:24 MST

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