Colleagues:
I wish to use 207Pb NMR to calibrate my MAS probes (Chemagnetics, circa
2000). However, I have a couple of questions:
a) What precautions should be used in handling the material? From the MSDS
data it is apparant a faceshield, gloves, and labcoat are advisable, but how
strong an oxidizer is it? Can it be packed into a rotor sandwiched between
Telfon tape without incident?
b) In the papers I have, no one seems to spin faster than 3 kHz. Is there a
problem spinning faster?
I will post any responses I receive.
Thanks,
Bill
--
Dr. W. L. Jarrett
University of Southern Mississippi
Department of Polymer Science
118 College Dr.
#10076
Hattiesburg, MS 39406-0076
Phone: (601)266-4551
Fax: (601)266-5504
Email: William.Jarrett_at_usm.edu
Received on Thu Nov 19 2009 - 12:53:23 MST