Hi all,
there are two minor problems in our laboratory (and maybe in other
labs too).
First of these problem is the phasing of ROESY spectra. It is
impossible to get a correct phase correction using only zero
and first order correction. There always remains a nonlinear
(maybe of second order) phase error of up to 2 degrees.
One possibility to cirumvent this problem is a much larger
spectrum width than necessary. But I believe, this is by no
means the ideal solution. Are there any better ideas?
The second problem is the simple pulse length determination.
Of course there are no technical problems, but it is time consuming
to determine all of the pulses (direct/inverse, hard/decoupling,
H-1, N-15, C-13, F2/F3/F4). The ideal solution would be an
automation program (fur Bruker spectrometers).
Is there maybe a ready prepared program available?
Thank you very much in advance for all hints.
Rainer
Received on Mon Nov 27 2000 - 09:12:43 MST