;hoesygpph_2.1 ;avance-version (13/08/06) ;2D heteronuclear NOE ;phase sensitive ; ;C. Yu & G. Levy, J. Am. Chem. Soc. 106, 6533 (1984) ; ;$CLASS=HighRes ;$DIM=2D ;$TYPE= ;$SUBTYPE= ;$COMMENT= #include #include #include "p2=p1*2" "p4=p3*2" "d12=20u" "d0=3u" "in0=inf1/2" "DELTA=d0*2+p2" "TAU=d8-p16-d16-54u" 1 ze 2 d1 do:f2 3 d12 pl2:f2 (p3 ph1):f2 DELTA (p4 ph5):f2 d0 p2 ph3 d0 (p3 ph2):f2 50u UNBLKGRAD TAU pl12:f2 p16:gp1 d16 4u BLKGRAD p1 ph4 go=2 ph31 cpd2:f2 d1 do:f2 mc #0 to 2 F1PH(ip1 & ip5, id0) exit ph1=0 ph2=0 2 ph3=0 0 2 2 ph4=0 0 0 0 1 1 1 1 2 2 2 2 3 3 3 3 ph5=1 ph31=0 2 0 2 1 3 1 3 2 0 2 0 3 1 3 1 ;pl1 : f1 channel - power level for pulse (default) ;pl2 : f2 channel - power level for pulse (default) ;pl12: f2 channel - power level for CPD/BB decoupling ;p1 : f1 channel - 90 degree high power pulse ;p2 : f1 channel - 180 degree high power pulse ;p3 : f2 channel - 90 degree high power pulse ;p4 : f2 channel - 180 degree high power pulse ;p16: homospoil/gradient pulse [1 msec] ;d0 : incremented delay (2D) [3 usec] ;d1 : relaxation delay; 1-5 * T1 ;d8 : mixing time ;d12: delay for power switching [20 usec] ;d16: delay for homospoil/gradient recovery ;inf1: 1/SW = 2 * DW ;in0: 1/(2 * SW) = DW ;nd0: 2 ;ns: 8 * n ;ds: 32 ;td1: number of experiments ;FnMODE: States-TPPI, TPPI, States or QSEQ ;cpd2: decoupling according to sequence defined by cpdprg2 ;pcpd2: f2 channel - 90 degree pulse for decoupling sequence ;for z-only gradients: ;gpz1: 30% ;use gradient files: ;gpnam1: SMSQ10.100 ;$Id: hoesygpph,v 1.1.4.2 2013/08/30 09:44:51 ber Exp $