Let me first thank everyone who responded to me.
Apparently my question created a great deal of confusion. I didn't mean to
imply that 2D's should be run spinning and I apologize for creating that
confusion. As we all know, they should be run with the spin turned off.
Where the problem originated was that the system was loosing its connection
when the spin turned off. I did learn that some of the Inova systems were
having this problem, but no one with a Mercury. My next step from here is
to get our service tech out to make certain nothing is going wrong
electronically.
Thanks again for all of the insights and information.
Adrienne
_____
> From: Hoeglund, Adrienne [mailto:AHoeglund_at_aoc-resins.com]
> Sent: Friday, March 18, 2005 12:18 PM
> To: 'AMMRL'
> Subject: Clarification - Glide/System Loosing Connection
Quick clarification.....my explanation below was not as clear as it should
have been and I apologize for that. When the system turns off the spinner,
it then looses connection with the console. If I kill acqproc and reboot
the console, turn the spinner back on and restart the experiment, the
spinner once again turns off but this time, does not loose connection to the
console. I am not having problems with the spinner turning off, I am having
problems with the system loosing its connection to the console when the spin
initially turns off. I hope that is a little clearer.
Thanks.
_____
> From: Hoeglund, Adrienne
> Sent: Friday, March 18, 2005 10:46 AM
> To: AMMRL
> Subject: Glide/System Loosing Connection
First let me thank everyone who responded to my question concerning the
Hetcor not running properly issue. What I discovered was the probe file had
not shared to that user for some reason. I re-distributed it to the system
and that fixed the problem (I figured he wasn't the only user affected).
The suggestion of HSQC was made rather than Hetcor. Also, thank you for the
suggestions of Chempack, it does sound quite nice. I will see if I can find
it.
Until then, I now have another completely different problem that is causing
me to wonder what is going on. When I set up an experiment to run a 2D
acquisition, the spinner will turn off and will lose connection to the
console. The first time it did this, I didn't notice and when I came back
had to reboot the console. So what I am doing now is stopping the
acquisition, restarting the spinner and then restarting the acquisition.
This method does take care of the problem if someone is around. I tend to
like to set up my 2D's overnight so that method won't work.
Has anyone else encountered this problem and if so, how have you resolved
it?
Thanks,
Adrienne
Adrienne B. Hoeglund
NMR Specialist
AOC, LLC.
950 Highway 57 East
Collierville, TN 38017
(901) 854-2800 ext. 532 - work
(901) 853-1582 - fax
www.aoc-resins.com
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Received on Mon Mar 21 2005 - 08:38:54 MST