Hello all--this is regarding our brand new (less than one month!) 500 MHz
Bruker system equipped with a BBFO cryo probe: we had an overnight power
outage, so the cryo platform warmed up. I cooled it down this morning;
there were no issues.
Unfortunately, the 13C S/N via the ATSM sample is only ~387 now. The proton
value was >2000, but I didn't check 31P etc. The tuning was normal.
Attaching a file here (acquisition parameters and spectrum for the 13C
SINO).
I'm still very new with taking care of Bruker systems, so I'd value any
advice and appreciate everyone's patience!
Thanks a lot in advance!
TJ.
Thusitha Jayasundera, Ph.D.
Director, Magnetic Resonance Center
Boston College
Merkert 105
2609 Beacon Street
Chestnut Hill MA 02467-3860
Tel: (617) 552-6984 (office)
Fax: (617) 552-2705 <617-552-2705>
Website: *https://www.bc.edu/bc-web/schools/mcas/departments/chemistry/research/facil-inst/nmr-center.html
<
https://www.bc.edu/bc-web/schools/mcas/departments/chemistry/research/facil-inst/nmr-center.html>*
Received on Fri Jun 24 2022 - 08:44:15 MST