Are your gradient pulses too long? I remember from a Bruker webinar that the
total duration of all gradient pulses in any DOSY sequence should not exceed
10 ms.
Best Regards,
Jürgen
_______________________________________________
Jürgen Schulte, Ph. D.
NMR Specialist
Binghamton University
SN Building, RM 1024
25 Murray Hill Road
Vestal, NY 13850
Ph.: 607-777-4405
Fax: 607-777-4478
schulte_at_binghamton.edu
http://nmr.binghamton.edu/Schulte.html
> From: main_at_ammrl.groups.io <main_at_ammrl.groups.io> On Behalf Of Yannick COPPEL
> Sent: Friday, December 8, 2023 11:50 AM
> To: main_at_ammrl.groups.io
> Subject: [External Email] Re: [AMMRL] Randomized response in the DOSY experiment
Dear Ryan,
We have tried with another probe and we observe the same problem. If this is
related with the gradient amplifier, I think we should also have some trouble
with 1D DOSY experiment and this is not the case.
Yannick
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Received on Fri Dec 08 2023 - 11:02:43 MST